Phenylacetyl chloride → HCID 13156314, compound

HRID 1447168Notes

Reaction equation

[CH:1]1[N:9]2[C:4]([NH:5][NH:6][C:7]3[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=32)=[N:3][N:2]=1.[C:14]1([CH2:20][C:21](Cl)=[O:22])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[C:14]1([CH2:20][C:21]([N:5]2[C:4]3=[N:3][N:2]=[CH:1][N:9]3[C:8]3[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=3[N:6]2[C:21](=[O:22])[CH2:20][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:22])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

Reactant 2

HCID 7679Phenylacetyl chloride

HCID 135503117HCID 135503117, compound

Product 1

HCID 13156314HCID 13156314, compoundYield 64%

Procedure

5 g (0.028 mole) of 4,5-dihydro-s-triazolo[3,4-c]benzo-as-triazine are reacted with 9.8 g (0.064 mole) of phenylacetyl chloride as described in Example 12. 7.33 g (64%) of the title compound are obtained; m.p.: 150°-151° C.

Sources & evidence

ORD record: ord-d9101e0b58934b32afa28f720a5d340b
Source dataset: uspto-grants-1982_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04316022

Reaction notes

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