HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1447180Generated: November 2, 2026
Benzyl azide → ethyl 1-benzyl-1H-tetrazole-5-carboxylate
https://huagongshe.com/reaction/1447180
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl azide | HCID 12152 | — |
| Reactant | Ethyl cyanoformate | HCID 69336 | — |
| Product | ethyl 1-benzyl-1H-tetrazole-5-carboxylate | HCID 12752368 | — |
Reaction Steps
An equimolar mixture of benzyl azide and ethyl cyanoformate is heated in a bomb under antogenous pressure at 150° C. for 4 hours. The resulting yellow oil is crystallized from hexane to give the title compound, m.p. 58°-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04316037 |
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| Source dataset | uspto-grants-1982_02 |
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| ORD ID | ord-b77491793d714df6a9a04190242037fa |
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| Source note | uspto-grants-1982_02 |
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