HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Phenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Benzene | HCID 241 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Product | Phenyl acetate | HCID 31229 | — |
Reaction Steps
The procedure of Example 1 is repeated except that 5 mmols of benzene are employed instead of the phenyl iodide of Example 1. Also, an additional 10 mls. of acetic acid solvent is employed. After the 4 hours of reaction at 75° C., no detectable phenyl acetate is formed. This again underscores the criticality of use of an aryl iodide of this invention as catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316045 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-476f727148d04a11b79665b7adff9711 |
| Source note | uspto-grants-1982_02 |