Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | 77770-13-9 | HCID 11450129 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 178482752 | HCID 178482752 | — |
Reaction Steps
319 mg of 2,6-di-tert-butyl-4-methylthiopyrylium perchlorate and 150 mg of 4-dimethylaminobenzaldehyde were heated in 5 ml of acetic anhydride for 40 minutes on an oil bath maintained at 100° C. After allowing to cool, diethyl ether was added to precipitate crystals and then the crystals were recrystallized from ethanol. Yield: 210 mg; m.p.: 240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04315983 |
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| Source dataset | uspto-grants-1982_02 |
|---|
| ORD ID | ord-2e095ee29c87417184b00f06245f237c |
|---|
| Source note | uspto-grants-1982_02 |
|---|
