HuagongsheHuagongshe Chemistry Print Report · For research reference only
epsilon-CAPROLACTONE → 1-Nonylazepan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | epsilon-CAPROLACTONE | HCID 10401 | — |
| Reactant | Nonylamine | HCID 16215 | — |
| Product | 1-Nonylazepan-2-one | HCID 12833263 | 26% |
Reaction Steps
Following example 5, heating 22.83 g (0.2 M) of 6-hexanolactone and 28.65 g (0.2 M) of 1-aminononane at 180° for 20 hours gave 11.5 g (26%) of product; b.p. 155°-165°/0.6 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316893 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-ddcec9f22e21478093f54db9ed52a2a4 |
| Source note | uspto-grants-1982_02 |