HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → (4-Chlorobenzyl)triphenylphosphonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | (4-Chlorobenzyl)triphenylphosphonium chloride | HCID 2733546 | — |
Reaction Steps
Triphenylphosphine (158 g., 0.60 mole) and 97 g. of 4-chlorobenzyl chloride are reacted in 800 ml. of boiling xylene according to the procedure of Example 25 (a) to yield 161 g. of colorless solid [(4-chlorophenyl)methyl]triphenylphosphonium chloride; m.p. 283°-285°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316905 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-13c7e16a6d9349509a2c1d6ea50cc033 |
| Source note | uspto-grants-1982_02 |