HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → Methyl Methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Potassium Persulfate | HCID 24412 | — |
| Reactant | Diethylaminoethyl Methacrylate | HCID 61012 | — |
| Reactant | Ethylene glycol diacrylate | HCID 75282 | — |
| Reactant | Emulphor | HCID 5364713 | — |
| Reactant | Sodium Bisulfite | HCID 23665763 | — |
| Solvent | Water | HCID 962 | — |
| Product | Methyl Methacrylate | HCID 6658 | — |
| Product | 2-(Diethylamino)ethyl acrylate | HCID 17050 | — |
Reaction Steps
50 Grams of N,N-diethylaminoethyl methacrylate, 50 g. of methyl methacrylate, 1 g. of Dupanol ME, 1 g. of Emulphor ON-870, 6 g. of ethylene diacrylate, 1 g. of potassium persulfate, and 0.5 g. of sodium bisulfite are dissolved or mixed with 1,000 g. of water. This mixture is tumbled in a water bath at 60° C. for 24 hr. to obtain a crosslinked copolymer of methyl methacrylate and N,N-diethylaminoethyl acrylate. The crosslinked polymer is separated from the aqueous dispersion by the method described in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177255 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-efb2909c87374da8ab769c9d65862d66 |
| Source note | uspto-grants-1979_12 |