HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → HCID 20384180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15854266 | HCID 15854266 | — |
| Product | HCID 20384180 | HCID 20384180 | — |
Reaction Steps
2-Carboxyphenoxathiin-10,10-dioxide, (0.50 g.) in carbon tetrachloride (25 ml.) and thionyl chloride (2.0 ml.) was boiled under reflux for 2 hr. The solvent was evaporated and methanol (20 ml.) added. The mixture was boiled under reflux for 20 min., and cooled, whereupon 2-methoxycarbonylphenoxathiin-10,10-dioxide crystallised out and was filtered off and dried, m.pt. 160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177257 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-485996e6b99345c38ab1dc8ff1c0a0b1 |
| Source note | uspto-grants-1979_12 |