HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylphosphoramide → Carbamic acid, (7-(phenylthio)imidazo(1,2-a)pyridin-2-yl)-,methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylphosphoramide | HCID 12679 | — |
| Reactant | HCID 13015361 | HCID 13015361 | — |
| Reactant | HCID 21202686 | HCID 21202686 | — |
| Product | Carbamic acid, (7-(phenylthio)imidazo(1,2-a)pyridin-2-yl)-,methyl ester | HCID 329368 | — |
Reaction Steps
A mixture of 2-amino 4-phenylthio pyridine, 1.0 g. (0.00494 mole) and 0.82 g. of methylchloroacetyl carbamate are heated in hexamethylphosphoramide following the procedures of Example 5 to yield 2(methoxycarbonylamino) 7-(phenylthio) imidazo [1,2-a] pyridine, m.p. 221°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177274 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-374076f87e4843b7b2ded0475b4baf44 |
| Source note | uspto-grants-1979_12 |