Dimethyl Sulfate → Carbamic acid, cyanomethyl-, ethyl ester

HRID 1447830Notes

Reaction equation

[CH2:1]([O:3][C:4]([NH:6][C:7]#[N:8])=[O:5])[CH3:2].[CH3:9]OS(OC)(=O)=O>>[CH2:1]([O:3][C:4]([N:6]([CH3:9])[C:7]#[N:8])=[O:5])[CH3:2]

Participants

Reactant 2

HCID 6497Dimethyl Sulfate

HCID 282131HCID 282131, compound

Product 1

HCID 109009Carbamic acid, cyanomethyl-, ethyl ester

Procedure

Berichte, 62, 1393-1394 (1929) discloses the reaction of the ethoxycarbonylcyanamide with dimethylsulfate to produce N-ethoxycarbonyl-N-methylcyanamide.

Sources & evidence

ORD record: ord-31072fc315264b1f8f008961078146cd
Source dataset: uspto-grants-1979_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04178448

Reaction notes

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