HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1-propanol → N-(2-hydroxy-1,1-dimethylethyl)-2-(isopropyl)-5-methylcyclohexanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1-propanol | HCID 11807 | — |
| Reactant | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| Product | N-(2-hydroxy-1,1-dimethylethyl)-2-(isopropyl)-5-methylcyclohexanecarboxamide | HCID 3016105 | — |
Reaction Steps
p-Menth-3-oyl chloride (3.0 g.) was reacted with 2-amino-2-methyl-propan-1-ol (3.0 g.) according to the procedure of Example 3. Product N-(1,1-dimethyl-2-hydroxyethyl)-p-menthane-3-carboxamide was obtained as a crystalline solid which was recrystallised from aqueous methanol. M.p. 123°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04178459 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-aff735b151a04e189e4dbb0a9c5020dc |
| Source note | uspto-grants-1979_12 |