HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p-Menthane-3-carboxylic acid | HCID 97896 | — |
| Reactant | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| Product | N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide | HCID 93591 | — |
Reaction Steps
Following the procedure of Example 5, p-menthane-3-carboxylic acid (1.84 g.) was reacted with thionyl chloride and the p-menth-3-oyl chloride then reacted with diethylamine (0.74 g.) in the presence of sodium hydroxide (0.4 g.). The product N,N-diethyl-p-menthane-3-carboxamide was recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04178459 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-90ce00b551b240ffa32aac7cf212334c |
| Source note | uspto-grants-1979_12 |