HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Ethylacetophenone → 3-Dimethylamino-4'-ethylacrylophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Ethylacetophenone | HCID 13642 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | 3-Dimethylamino-4'-ethylacrylophenone | HCID 53833899 | — |
Reaction Steps
A mixture of 50 g. of 4'-ethylacetophenone and 50 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. Evaporation gave a thick oil which crystallized on the addition of hexane, m.p. 80°-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04178449 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-63fd5dd7d8ac4491946c9a8f19e9106d |
| Source note | uspto-grants-1979_12 |