HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-alpha-tetralone → HCID 54253203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-alpha-tetralone | HCID 14112 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-[3-(Dimethylamino)propoxy]benzaldehyde | HCID 546932 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54253203 | HCID 54253203 | 81.4% |
Reaction Steps
Interaction of 16 g of 6-methoxy-1-tetralone and 19 g of 4-(3-dimethylaminopropoxy)benzaldehyde in 95 ml of ethanol in the presence of 0.6 g of potassium hydroxide following the procedure described in Example 1A, yields 27 g of crude product; melting point 68-71° C. Following crystallization from 70 ml of diisopropyl ether, the product weighs 18.6 g, melting point 76°-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04179558 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-aa843d977a00416d9d2bdca805de6768 |
| Source note | uspto-grants-1979_12 |