HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 20382001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methoxybenzyl bromide | HCID 165021 | — |
| Reactant | Pirquinozol | HCID 135449340 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20382001 | HCID 20382001 | — |
Reaction Steps
210 g of p-methoxybenzyl bromide and 40 g of potassium iodide are added to 114 g of 2-(hydroxymethyl)pyrazolo[1,5-c]quinazolin-5(6H)-one and 276 g of potassium carbonate in 2 l. of methanol. After refluxing for 5 hours, the reaction is cooled, poured into 6 l. of water and the title compound is filtered off and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04179561 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-9c607960161e439e9867f2d7cc3a9a2d |
| Source note | uspto-grants-1979_12 |