Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | HCID 12298183 | HCID 12298183 | — |
| Product | HCID 12298069 | HCID 12298069 | — |
Reaction Steps
A mixture of 3.34 parts of (2-bromoethyl)benzene, 4.80 parts of propyl 4-[N-(1-oxopropyl)-N-phenylamino]-4-piperidinecarboxylate, 2.02 parts of N,N-diethylethanamine and 81 parts of N,N-dimethylacetamide is stirred and heated for 3 hours at 70°-80° C. The reaction mixture is cooled and poured onto 400 parts of water. The product is extracted with 1,1'-oxybisethane. The extract is washed with water, dried, filtered and evaporated. The oily residue is purified by column-chromatography over silica gel using a mixture of trichloromethane and 15% of methanol as eluent. The pure fractions are collected and the eluent is evaporated. The residue is converted into the ethanedioate salt in 2-propanone, yielding propyl 4-[N-(1-oxopropyl)-N-phenylamino]-1-(2-phenylethyl)-4-piperidinecarboxylate ethanedioate; mp. 215.7° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04179569 |
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| Source dataset | uspto-grants-1979_12 |
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| ORD ID | ord-8bc004007bd64acf9f78c8afec58483f |
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| Source note | uspto-grants-1979_12 |
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