HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → p-(2,4-Dimethoxybenzyloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | p-(2,4-Dimethoxybenzyloxy)acetanilide | HCID 20379816 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | p-(2,4-Dimethoxybenzyloxy)aniline | HCID 20379808 | — |
Reaction Steps
p-(2,4-Dimethoxybenzyloxy)acetanilide (3 g, 0.01 M) in ethanol (30 ml) is treated with potassium hydroxide (3 g), then the mixture is heated under reflux for 12 hours. The solvent is removed by evaporation, the residue treated with water and extracted with ether. The ether solution is treated with charcoal, dried and concentrated to afford p-(2,4-dimethoxybenzyloxy)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04180509 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-b8a49b87ed4243e9aa697cc303af4aa9 |
| Source note | uspto-grants-1979_12 |