HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → Butyl 4-(tert-butylperoxy)-4-methylpentan-2-yl carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | HCID 19612317 | HCID 19612317 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Butyl 4-(tert-butylperoxy)-4-methylpentan-2-yl carbonate | HCID 23346606 | — |
Reaction Steps
To a solution of 8.1 g. (0.11 mole) of n-butyl alcohol and 7.9 g. (0.1 mole) of pyridine in diethyl ether cooled to 10°±1° C. was added a solution of 27.0 g. (0.1 mole) 1,3-dimethyl-3-(t-butylperoxy)butyl chloroformate. The reaction temperature was controlled at 15°±1° C. during the addition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04180518 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-ce5598552d554ba4a491b9b6a5f9c3cc |
| Source note | uspto-grants-1979_12 |