HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → N,N-dimethyl-(3,4-dibromophenyl)trimethylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 3-(Dimethylamino)propyl chloride hydrochloride | HCID 94308 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 3,4-Dibromoaniline | HCID 521981 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N,N-dimethyl-(3,4-dibromophenyl)trimethylenediamine | HCID 20376385 | — |
Reaction Steps
In the manner given in Example 1, 3,4-dibromoaniline, 1-chloro-3-dimethylaminopropane hydrochloride, sodium carbonate and sodium bicarbonate are heated in toluene to give N,N-dimethyl-(3,4-dibromophenyl)trimethylenediamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04180522 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-7b901112f2594f4c9ed16c6daa437e49 |
| Source note | uspto-grants-1979_12 |