Borane → HCID 20376392, compound

HRID 1448456Notes

Reaction equation

HRID 1448456 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[Cl:17])[NH:5][CH2:6][CH2:7][CH2:8][C:9]([N:11]([CH3:13])[CH3:12])=O.B>>[Cl:1][C:2]1[CH:3]=[C:4]([NH:5][CH2:6][CH2:7][CH2:8][CH2:9][N:11]([CH3:13])[CH3:12])[CH:14]=[CH:15][C:16]=1[Cl:17]

Participants

3

Reactant 2

HCID 6331BoraneHCID 20376429HCID 20376429, compound

Product 1

HCID 20376392HCID 20376392, compound

Procedure

In the manner given in Example 24, 4-(3',4'-dichloroanilino)-N,N-dimethylbutyramide is reduced with borane in tetrahydrofuarn to give N-(3',4'-dichlorophenyl)-N',N'-dimethylbutane-1,4-diamine as an oil.

Sources & evidence

ORD record
ord-b562c55679c140f8846ba453b1e22569
Source dataset
uspto-grants-1979_12
Patent number
US04180522

Reaction notes

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