Diethyl Ether → HCID 22691450, compound

Participants

Reaction Steps

5 g of N-benzyloxycarbonyl-L-proline n-pentylamide were dissolved in 20 ml of 4-N hydrogen bromide in acetic acid and the mixture was stirred for 1 hour. 150 ml of dry ether were then added. A clear oil precipitated out and was allowed to settle. The ether was decanted off and the oil washed with a further 100 ml of dry ether. Evaporation yielded 3.4 g (82%) of L-proline n-pentylamide in the form of an oil.

Provenance & Evidence