HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 20375651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | HCID 12673483 | HCID 12673483 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20375651 | HCID 20375651 | — |
Reaction Steps
To a solution of 1 g of 3-(2-fluorophenoxy) pyridine in 40 ml of acetonitrile is added 0.9 g of ethyl bromoacetate and the solution is refluxed 16 hours. The solvent is removed in vacuo to yield 1-(2-ethoxy-2-oxoethyl)-3-(2-fluorophenoxy) pyridinium bromide; mp 133°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04187311 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-72c3c2dd40f14866b1bfb32b4220dc7b |
| Source note | uspto-grants-1980_02 |