Ethanol → HCID 20375722, compound

HRID 1448810Notes

Reaction equation

HRID 1448810 reaction equation
[ClH:1].[NH2:2][CH:3]1[CH2:8][CH:7]=[CH:6][C:5]([C:9]([OH:11])=[O:10])=[CH:4]1.[CH2:12](O)[CH3:13]>>[ClH:1].[NH2:2][CH:3]1[CH2:8][CH:7]=[CH:6][C:5]([C:9]([O:11][CH2:12][CH3:13])=[O:10])=[CH:4]1

Participants

3

Reactant 2

HCID 702EthanolHCID 70583694HCID 70583694, compound

Product 1

HCID 20375722HCID 20375722, compound

Conditions

Temperature
0 °C

Procedure

3-Amino-1,5-cyclohexadiene carboxylic acid hydrochloride (200 mg) is dissolved in ethanol containing anhydrous HCl, and the resulting solution is stirred over night at 0° C. Evaporation of the solvent affords ethyl 3-amino-1,5-cyclohexadienecarboxylate hydrochloride.

Workup

  1. customEvaporation of the solvent

Sources & evidence

ORD record
ord-d2d2c5b74260498e9aa1b5ea4f56be8b
Source dataset
uspto-grants-1980_02
Patent number
US04187316

Reaction notes

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