HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 594510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 14416083 | HCID 14416083 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 594510 | HCID 594510 | 61% |
Reaction Steps
6-Chloro-9-(2,6-dichlorobenzyl)purine (314 mg), 365 mg of diethylamine and 25 ml of methanol were treated in the same manner as Example 2, whereby 212 mg (yield 61%) of 9-(2,6-dichlorobenzyl)-6-diethylaminopurine was obtained as needles melting at 140°-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04189485 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-b219050172424d58a5ca384856a0d991 |
| Source note | uspto-grants-1980_02 |