HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 53838392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | Lithium Bromide | HCID 82050 | — |
| Reactant | HCID 23455750 | HCID 23455750 | — |
| Catalyst | Zinc bromide | HCID 10421208 | — |
| Product | HCID 53838392 | HCID 53838392 | — |
Reaction Steps
6-(4-Methoxyphenyl)-3-hexenyl bromide [V; Ar is 4-CH3OC6H4, R is H] was prepared from 38.2 g. of 2-(4-methoxyphenyl)ethyl cyclopropyl carbinol (Preparation B5), 42.5 g. of phosphorus tribromide, 35 g. of lithium bromide and 40 g. of zinc bromide according to the procedure given above in Preparation C1, affording 48 g. of product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04189500 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-4e75917dc0404eb4a50f9d4b336b0508 |
| Source note | uspto-grants-1980_02 |