HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 54042329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | Lithium Bromide | HCID 82050 | — |
| Reactant | HCID 23455733 | HCID 23455733 | — |
| Catalyst | Zinc bromide | HCID 10421208 | — |
| Product | HCID 54042329 | HCID 54042329 | — |
Reaction Steps
6-(4-Chlorophenyl)-3-hexenyl bromide [V; Ar is 4-ClC6H4, R is H] was prepared from 21 g. of 2-(4-chlorophenyl)ethyl cyclopropyl carbinol (Preparation B7), 23 g. of phosphorus tribromide, 18.85 g. of lithium bromide and 22.5 g. of zinc bromide according to the procedure given above in Preparation C1, affording 25.5 g. of product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04189500 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-3506065cd4dc4000bb148d3606835c8e |
| Source note | uspto-grants-1980_02 |