HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → 4-Benzoyloxy-1-octyne
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 1-Octyn-4-ol | HCID 103656 | — |
| Product | 4-Benzoyloxy-1-octyne | HCID 20442054 | — |
Reaction Steps
From fractions 13-20 is obtained 75 mg of colorless oil, identical to 4-hydroxy-1-octyne, [α]D25 =-17±1.0° (C=0.77, ethyl acetate). This compound has the (R)-configuration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04189597 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-e9e38c84621448abab87a452ec0e60b7 |
| Source note | uspto-grants-1980_02 |