Sulfuric Acid → HCID 86736849, compound

Participants

Reaction Steps

A sample of 7.8 grams of 3-methoxy-3-t-butyl-4-neopentyl 1,2 dithiole was dissolved in 16 grams of ether. To the mixture was slowly added 3.0 grams of concentrated sulfuric acid. After the exothermic reaction was completed, the solid precipitate was filtered off and there was isolated 10.1 grams (93.8% of theory) of 4-neopentyl-3-t-butyl 1,2 dithiolium hydrogen sulfate.

Provenance & Evidence