Methanol → HCID 22869565, compound

Participants

Reaction Steps

K2CO3 (20 mg, 0.145 mmol) was added to a stirred solution of 3 (100 mg, 0.131 mmol) in CH3OH (2 mL). After 30 min, the reaction mixture was filtered, diluted with ether (10 mL), and washed with aq NH4Cl and brine. Concentration followed by flash chromatography (20% diethyl ether/pentane) afforded N-Boc-O-allyltyrosine methyl ester (40.0 mg, 92%).

Provenance & Evidence