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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1449714생성일: 2026년 10월 25일

1-[5-Chloro-4-(1-methylethyl)amino-3-pyridazinyl]piperazine → 1-[4-(1-Methylethyl)amino-3-pyridazinyl]piperazine

https://huagongshe.com/reaction/1449714

반응식

참여 물질

역할이름HCID투입량
반응물1-[5-Chloro-4-(1-methylethyl)amino-3-pyridazinyl]piperazineHCID 21477673—
용매TriethylamineHCID 8471—
생성물1-[4-(1-Methylethyl)amino-3-pyridazinyl]piperazineHCID 21477613—

반응 단계

Following the general procedure of PREPARATION 10 and making non-critical variations but starting with 1-[5-chloro-4-(1-methylethyl)amino-3-pyridazinyl]piperazine (PREPARATION 42, 1.7 g) and triethylamine (0.81 g), the title compound is obtained, NMR (CDCl3) 1.28, 2.06, 3.05, 3.11, 3.59, 4.75, 6.39, and 8.49 δ; CMR (CDCl3) 22.2, 43.2, 46.2, 50.6, 103.7, 138.7, 148.4 and 154.5 δ.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05599930
출처 데이터셋uspto-grants-1997_02
ORD IDord-da9449ee7b764653bb6950a4255dfb82
출처 메모uspto-grants-1997_02