HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13819307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | tert-Butoxycarbonyl-L-isoleucine | HCID 2724762 | — |
| Product | HCID 13819307 | HCID 13819307 | — |
Reaction Steps
The title compound was prepared by the method of Example 8 using ethyl iodide (0.4 mL, 5 mmol) instead of methyl iodide and BOC--L--Ile--OH--0.5 H2O (1.0 g, 4 mmol) instead of the title product of Example 1. Concentration afforded the title compound (1.1 g) as a water white liquid and the structure verified by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599947 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-5fb5409f0af9485399a81dca24f44464 |
| Source note | uspto-grants-1997_02 |