HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 131719822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Boc-D-isoleucine | HCID 6992552 | — |
| Product | HCID 131719822 | HCID 131719822 | — |
Reaction Steps
The title compound was prepared by the method of Example 8 using ethyl iodide (0.4 mL, 5 mmol) instead of methyl iodide and BOC--D--Ile--OH--0.5 H2O (1.0 g, 4 mmol) instead of the title product of Example 1. Concentration afforded the title compound (1.2 g) as a water white liquid and the structure verified by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599947 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-222c7fa1e0ce4d8d9347f012f3c3348b |
| Source note | uspto-grants-1997_02 |