4-Phenylbutyric Acid → HCID 54111269, compound

HRID 1449805Notes

Reaction equation

HRID 1449805 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][OH:8].[C:9]1([CH2:15][CH2:16][CH2:17][C:18](O)=[O:19])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:18](=[O:19])[CH2:17][CH2:16][CH2:15][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 47754-Phenylbutyric AcidHCID 779706-Bromo-1-hexanol

Product 1

HCID 54111269HCID 54111269, compoundYield 72%

Procedure

From 6-bromo-1-hexanol and 4-phenylbutyric acid. Working up by means of distillation. Yield: 72%. Boiling point: 158° C. (0.01 mbar)

Workup

  1. distillationWorking up by means of distillation

Sources & evidence

ORD record
ord-2d8caaad658e4e50b7656cac9f8ecf99
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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