6-Bromohexanoic acid → HCID 54005044, compound

HRID 1449806Notes

Reaction equation

HRID 1449806 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].[C:10]1([CH2:16][CH2:17][CH2:18][CH2:19]O)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:10]1([CH2:16][CH2:17][CH2:18][CH2:19][O:8][C:7](=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][Br:1])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 202106-Bromohexanoic acidHCID 76889Benzenebutanol

Product 1

HCID 54005044HCID 54005044, compoundYield 80%

Procedure

From 6-bromocaproic acid and 4-phenyl-1-butanol. Working up by means of distillation. Yield: 80%. Boiling point: 158° C. (0.008 mbar).

Workup

  1. distillationWorking up by means of distillation

Sources & evidence

ORD record
ord-9d63ec2b5eac40e389aedfc7d457e2c1
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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