3-(4-Hydroxyphenyl)propionic acid → HCID 86750279, compound

HRID 1449810Notes

Reaction equation

HRID 1449810 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][OH:8].[OH:9][C:10]1[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][C:18](O)=[O:19])=[CH:12][CH:11]=1>>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:18](=[O:19])[CH2:17][CH2:16][C:13]1[CH:14]=[CH:15][C:10]([OH:9])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 103943-(4-Hydroxyphenyl)propionic acidHCID 779706-Bromo-1-hexanol

Product 1

HCID 86750279HCID 86750279, compoundYield 70%

Procedure

From 6-bromo-1-hexanol and 3-(4-hydroxyphenyl)propionic acid. Working up by means of distillation. Yield: 70%. Boiling point: 205° C. (0.05 mbar).

Workup

  1. distillationWorking up by means of distillation

Sources & evidence

ORD record
ord-cbec55b7cbe643ccac8362f02a4f344d
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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