6-Amino-1-hexanol → HCID 23352640, compound

HRID 1449812Notes

Reaction equation

HRID 1449812 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[CH:4]1[O:6][CH2:5]1.[NH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18]>C(OCC)(=O)C.CO>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[CH:4]([OH:6])[CH2:5][NH:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18]

Participants

4

Reactant 2

HCID 199606-Amino-1-hexanolHCID 5607092-(2-Chlorophenyl)oxirane

Product 1

HCID 23352640HCID 23352640, compoundYield 41%

Reagents, catalysts & solvents 1

HCID 21584119Ethylacetate methanolSolvent

Procedure

From 2-chlorostyrene oxide and 6-amino-1-hexanol. Working up by means of chromatography (ethyl acetate/methanol 1:1). Yield: 41%.

Sources & evidence

ORD record
ord-71e7522ee2de493e96a00da81cc3eafa
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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