HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 23352577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzenemethanol, 4-amino-alpha-(aminomethyl)-3,5-dichloro- | HCID 217242 | — |
| Reactant | HCID 54348980 | HCID 54348980 | — |
| Solvent | Ethyl acetate methanol triethylamine | HCID 21980445 | — |
| Product | HCID 23352577 | HCID 23352577 | — |
Reaction Steps
According to method I (dimethylformamide, 2 hours at 90° C.) from 2-amino-1-(4-amino-3,5-dichlorophenyl)ethanol and {2-(1-naphthyl)ethyl}6-bromohexanoate. Working up by means of chromatography (ethyl acetate/methanol/triethylamine 16:2:1). Recrystallized as the free base from ethyl acetate. Melting point: 60°-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-3674816cbbae4d6c92dfc98bcee8e81a |
| Source note | uspto-grants-1997_02 |