HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 131719824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzenemethanol, 4-amino-alpha-(aminomethyl)-3,5-dichloro- | HCID 217242 | — |
| Reactant | HCID 53657044 | HCID 53657044 | — |
| Solvent | Ethyl acetate methanol triethylamine | HCID 21980445 | — |
| Product | HCID 131719824 | HCID 131719824 | — |
Reaction Steps
According to method I (dimethylformamide, 3 hours at 90° C.) from (6-bromo-1-hexyl) 3-fluorophenylacetate and 2-amino-1-(4-amino-3,5-dichlorophenyl)ethanol. Working up by means of chromatography (ethyl acetate/methanol/triethylamine 16:2:1). Recrystallized as the oxalate from acetone. Melting point: 70°-71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-b28f6d84706240e3ab6405947da80dbd |
| Source note | uspto-grants-1997_02 |