HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86750296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzenemethanol, 4-amino-alpha-(aminomethyl)-3,5-dichloro- | HCID 217242 | — |
| Reactant | HCID 53838732 | HCID 53838732 | — |
| Solvent | Ethyl acetate methanol triethylamine | HCID 21980445 | — |
| Product | HCID 86750296 | HCID 86750296 | — |
Reaction Steps
According to method I (dimethylformamide, 3 hours at 90° C.) from (6-bromo-1-hexyl)3-phenylbutanoate and 2-amino-1-(4-amino-3,5-dichlorophenyl)ethanol. Working up by means of chromatography (ethyl acetate/methanol/triethylamine 20:2:1). Recrystallized as the maleate from ethyl acetate. Melting point: 51°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-6c70a0c425234736a94ecea23278e217 |
| Source note | uspto-grants-1997_02 |