N-vinyl-2-pyrrolidone → N,N-Diethylacrylamide

HRID 1450027Notes

Reaction equation

HRID 1450027 reaction equation
[CH2:1]([NH:4][C:5](=[O:8])[CH:6]=[CH2:7])[CH2:2]C.[CH:9](N1CCCC1=O)=[CH2:10]>>[CH2:1]([N:4]([CH2:9][CH3:10])[C:5](=[O:8])[CH:6]=[CH2:7])[CH3:2]

Participants

3

Reactant 2

HCID 6917N-vinyl-2-pyrrolidoneHCID 114794N-(n-Propyl) acrylamide

Product 1

HCID 17583N,N-Diethylacrylamide

Procedure

N-n-propylacrylamide (NnPAM) and vinylpyrrolidone were purchased from a commercial vendor and used as received. Anhydrous methanol was degassed by vigorously bubbling dry nitrogen through it.

Workup

  1. customAnhydrous methanol was degassed
  2. customby vigorously bubbling dry nitrogen through it

Sources & evidence

ORD record
ord-26db2db21b8b48bf812c0b8ac4c09465
Source dataset
uspto-grants-1997_02
Patent number
US05600044

Reaction notes

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