HRID1450099

反应详情

EQUATION

反应方程式

HRID 1450099 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A sample (548 mg) of the compound from step 470d was dissolved in methanol, 140 mg of 10% Pd/C was added, and the mixture was hydrogenated at 4 arm H2 for 42 hours at room temperature. The solution was filtered, and the solvent was removed to give 140 mg of the title compound.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. customthe solvent was removed