HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol hydrochloride → trans-(+/-)-Tetrahydro-4-mercapto-2-furanmethanol 2-carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol hydrochloride | HCID 21912024 | — |
| Reactant | Ethanethioic acid trans-(+/-)-S-[5-[[(aminocarbonyl)oxy]methyl]tetrahydro-3-furanyl]ester | HCID 86752560 | — |
| Reactant | Methoxide methyl alcohol | HCID 131719842 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | trans-(+/-)-Tetrahydro-4-mercapto-2-furanmethanol 2-carbamate | HCID 130972113 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 16 using 0.109 g of product from Example 7, 120 microliter of 25% methoxide/methyl alcohol, 1.75 ml of tetrahydrofuran, 280 microliter of 1.86N hydrochloric acid/isopropyl alcohol to give the desired product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602118 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-d39f64de694d460a9da1fc3496f012e2 |
| Source note | uspto-grants-1997_02 |