HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → (3R-trans)-Tetrahydro-4-[(methylsulfonyl)oxy]-3-furancarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 188069-24-1 | HCID 86750346 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | (3R-trans)-Tetrahydro-4-[(methylsulfonyl)oxy]-3-furancarbonitrile | HCID 54080273 | 89.3% |
Reaction Steps
The title compound is prepared by the procedure of Example 178 using 0.367 g of product from Example 197, 0.394 g of triethylamine, and 0.446 g of methanesulfonyl chloride to give 0.554 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602118 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-3f4f4fba07cd4c1d9cbb8977c57a5005 |
| Source note | uspto-grants-1997_02 |