HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 88378301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 67707322 | HCID 67707322 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 88378301 | HCID 88378301 | 73.3% |
Reaction Steps
The title compound is prepared by the procedure of Example 202 using 0.462 g of product from Example 326, 12 ml of 80% aqueous acetic acid, 0.187 g of anisole, and 0.443 g of mercuric trifluoroacetate to give after chromatography (Silica gel: 50-80% ethyl acetate/hexane) 0.248 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602118 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-0eb4b3132bcc447e836a2a45cabb1533 |
| Source note | uspto-grants-1997_02 |