HRID1450377

反应详情

EQUATION

反应方程式

HRID 1450377 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.4 g (7.7 mmol) of the chloride from Example 1, Step B and 1.5 g (7.7 mmol) 4-Amino-2'-cyanobiphenyl were heated in 30 ml dry ethanol for 5 h. After removal of the solvent in vacuo the nitrile was obtained in colorless crystals from ethanol, m.p. 247°-248° C.

WORKUP

后处理

  1. customAfter removal of the solvent in vacuo the nitrile
  2. customwas obtained in colorless crystals from ethanol, m.p. 247°-248° C.