HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1450630Generated: November 3, 2026
Potassium Hydroxide → 5-(3-Buten-1-ynyl)-2,2'-bithienyl
https://huagongshe.com/reaction/1450630
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 18920422 | HCID 18920422 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(3-Buten-1-ynyl)-2,2'-bithienyl | HCID 70813 | — |
Reaction Steps
5-(4-chloro-1-butynyl)-2,2'-bithiophene was dissolved in ethanol. KOH dissolved in ethanol was then added in and heated at 75° C. for 15 minutes. The remaining process was as described in procedure(a) and the same product was obtained. The yield was above 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05602170 |
|---|
| Source dataset | uspto-grants-1997_02 |
|---|
| ORD ID | ord-e338310b36e945fbab9c7afe1aabe134 |
|---|
| Source note | uspto-grants-1997_02 |
|---|
