HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 18920425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 3-Butyn-1-ol, 4-(5-(2-thienyl)-2-thienyl)- | HCID 440357 | — |
| Solvent | Acetate | HCID 175 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18920425 | HCID 18920425 | — |
Reaction Steps
0.8 g of 5-(4-hydroxy-1-butynyl)-2,2 '-bithiophene was dissolved in 8 ml of pyridine. 1 ml of benzoyl chloride was added at room temperature, stirred for few minutes and kept overnight. The reaction mixture was treated as in acetate example 81. Slightly yellowish crystal was then obtained and the melting point thereof was 61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602170 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-070145137a0f4fecbaa35cda904e7af1 |
| Source note | uspto-grants-1997_02 |