HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 19358829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 19358835 | HCID 19358835 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19358829 | HCID 19358829 | — |
Reaction Steps
The compound of Example 6 (5 g, 15 mmol) is heated with 50 g of imidazole at 200° C. under N2 for 16 h. The reaction mixture is cooled to ~100° C., and 150 mL methanol is added. The solids are filtered and washed with methanol to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602252 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-3b2f5d8ca284493886704e1bcaabc9b8 |
| Source note | uspto-grants-1997_02 |