Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 2-Hydrazinyl-5-nitropyridine | HCID 4031931 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 95913 | HCID 95913 | 62% |
Reaction Steps
In 20 ml of ethanol were dispersed 1.59 g of 2-hydrazino-5-nitropyridine and 1.13 g of benzaldehyde. The dispersion was refluxed at 100° C. for 16.5 hours. The reaction solution was allowed to cool at room temperature. The resulting precipitate was collected by suction filtration, washed with ethanol and air dried, obtaining 1.55 g (yield 62%) of orange yellow fine acicular crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05604004 |
|---|
| Source dataset | uspto-grants-1997_02 |
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| ORD ID | ord-4d53fe24556546c494b3ac612a277c0b |
|---|
| Source note | uspto-grants-1997_02 |
|---|
