HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratrylamine → HCID 19974378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratrylamine | HCID 79832 | — |
| Reactant | HCID 19974382 | HCID 19974382 | — |
| Solvent | 1,4-Dioxane--water (1/1) | HCID 21886435 | — |
| Product | HCID 19974378 | HCID 19974378 | 61.6% |
Reaction Steps
1.5 g of 4,5-dibromo-6-[2-(4-nitrophenylthio)ethyloxy]-3(2H)-pyridazinone and 1.32 g of 3,4-dimethoxyphenylmethyl amine were disolved in water-dioxane (1:1) and refluxed for 7 hr. The reaction mixture was cooled to room temperature. The resulting crystals was collected by filtration and recrystallized from dioxane to give 1.1 g of the objective compound. Yield, 60%, Melting point, 170°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604226 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-9631890bdd3645f399be29842a78d95b |
| Source note | uspto-grants-1997_02 |